Information card for entry 2227906

Structure parameters

• Chemical name: Oxido{<i>N</i>-[(2-oxido-1-naphthyl-κ<i>O</i>)methylidene]asparaginato- κ^2^<i>O</i>^1^,<i>N</i>^2^}(1,10-phenanthroline- κ^2^<i>N</i>,<i>N</i>')vanadium(IV) <i>N</i>,<i>N</i>-dimethylformamide monosolvate
• Formula: C30 H27 N5 O6 V
• Calculated formula: C30 H27 N5 O6 V
• Title of publication: Oxido{<i>N</i>-[(2-oxido-1-naphthyl-κ<i>O</i>)methylidene]asparaginato-κ^2^<i>O</i>^1^,<i>N</i>^2^}(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')vanadium(IV) <i>N</i>,<i>N</i>-dimethylformamide monosolvate
• Authors of publication: Bian, Lin; Li, Lianzhi; Zhang, Qingfu; Wang, Daqi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 9
• Pages of publication: m1051
• a: 10.357 ± 0.001 Å
• b: 11.1021 ± 0.0012 Å
• c: 12.9119 ± 0.0014 Å
• α: 101.396 ± 0.002°
• β: 104.196 ± 0.002°
• γ: 91.01 ± 0.001°
• Cell volume: 1407.5 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.1867
• Weighted residual factors for all reflections included in the refinement: 0.2162
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes