Information card for entry 2230027

Structure parameters

• Common name: Poly[[([2.2.2]-cryptand)rubidium] [[(18-crown-6)rubidium]dirubidiumnonastannide] pentaammonia]
• Chemical name: Poly[[(4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane)rubidium] [[(1,4,7,10,13,16-hexaoxacyclooctadecane)rubidium]di-μ-rubidium-μ- nonastannide] pentaammonia]
• Formula: C30 H75 N7 O12 Rb4 Sn9
• Calculated formula: C30 H72 N7 O12 Rb4 Sn9
• Title of publication: [Rb(18-crown-6)][Rb([2.2.2]-cryptand)]Rb~2~Sn~9~·5NH~3~
• Authors of publication: Gaertner, Stefanie; Korber, Nikolaus
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 5
• Pages of publication: m613 - m614
• a: 10.79 ± 0.002 Å
• b: 15.6 ± 0.003 Å
• c: 36.96 ± 0.007 Å
• α: 90°
• β: 91.2 ± 0.03°
• γ: 90°
• Cell volume: 6220 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1069
• Weighted residual factors for all reflections included in the refinement: 0.1117
• Goodness-of-fit parameter for all reflections included in the refinement: 0.835
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes