Information card for entry 2233399

Structure parameters

• Chemical name: {2-[Bis(2,4-di-<i>tert</i>-butylphenoxy)phosphanyloxy-κ<i>P</i>]-3,5-di- <i>tert</i>-butylphenyl-κ<i>C</i>^1^}[(1,2,5,6-η)-cycloocta-1,5- diene]rhodium(I) toluene monosolvate
• Formula: C57 H82 O3 P Rh
• Calculated formula: C57 H82 O3 P Rh
• Title of publication: {2-[Bis(2,4-di-<i>tert</i>-butylphenoxy)phosphanyloxy-κ<i>P</i>]-3,5-di-<i>tert</i>-butylphenyl-κ<i>C</i>^1^}[(1,2,5,6-η)-cycloocta-1,5-diene]rhodium(I) toluene monosolvate
• Authors of publication: Selent, Detlef; Spannenberg, Anke; Börner, Armin
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 2
• Pages of publication: m215
• a: 11.1212 ± 0.0003 Å
• b: 12.5865 ± 0.0003 Å
• c: 20.069 ± 0.0005 Å
• α: 106.891 ± 0.001°
• β: 102.344 ± 0.001°
• γ: 94.483 ± 0.001°
• Cell volume: 2596.13 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0666
• Weighted residual factors for all reflections included in the refinement: 0.0691
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes