Information card for entry 2235024

Structure parameters

• Chemical name: <i>N</i>,<i>N</i>'-Dibutyl-<i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'- tetramethylethane-1,2-diaminium μ-oxido-bis[trichloridoferrate(III)]
• Formula: C14 H34 Cl6 Fe2 N2 O
• Calculated formula: C14 H34 Cl6 Fe2 N2 O
• Title of publication: <i>N</i>,<i>N</i>'-Dibutyl-<i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'-tetramethylethane-1,2-diaminium μ-oxido-bis[trichloridoferrate(III)]
• Authors of publication: Närhi, Sari M.; Kostamo, Jatta; Asikkala, Janne; Oilunkaniemi, Raija; Laitinen, Risto S.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 6
• Pages of publication: m748
• a: 8.9803 ± 0.0018 Å
• b: 14.689 ± 0.003 Å
• c: 19.249 ± 0.004 Å
• α: 81.75 ± 0.03°
• β: 87.66 ± 0.03°
• γ: 80.32 ± 0.03°
• Cell volume: 2476.7 ± 0.9 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0566
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1127
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes