Crystal structures of methyl 3-(4-isopropylphenyl)-1-methyl-1,2,3,3a,4,9b-hexahydrothiochromeno[4,3-<i>b</i>]pyrrole-3a-carboxylate, methyl 1-methyl-3-(<i>o</i>-tolyl)-1,2,3,3a,4,9b-hexahydrothiochromeno[4,3-<i>b</i>]pyrrole-3a-carboxylate and methyl 1-methyl-3-(<i>o</i>-tolyl)-3,3a,4,9b-tetrahydro-1<i>H</i>-thiochromeno[4,3-<i>c</i>]isoxazole-3a-carboxylate
Authors of publication
Raja, R.; Suresh, M.; Raghunathan, R.; SubbiahPandi, A.
Journal of publication
Acta Crystallographica Section E
Year of publication
2015
Journal volume
71
Journal issue
6
Pages of publication
574 - 577
a
10.733 ± 0.0003 Å
b
7.7568 ± 0.0002 Å
c
24.9436 ± 0.0007 Å
α
90°
β
98.485 ± 0.001°
γ
90°
Cell volume
2053.92 ± 0.1 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.047
Residual factor for significantly intense reflections
0.0407
Weighted residual factors for significantly intense reflections
0.1055
Weighted residual factors for all reflections included in the refinement
0.1109
Goodness-of-fit parameter for all reflections included in the refinement
