Information card for entry 2241764

Structure parameters

• Chemical name: Bis{(<i>E</i>)-1-[(2,4,6-tribromophenyl)diazenyl]naphthalen-2-olato}nickel(II)
• Formula: C32 H16 Br6 N4 Ni O2
• Calculated formula: C32 H16 Br6 N4 Ni O2
• SMILES: c1(c(cc(cc1Br)Br)Br)[N]1=Nc2c(ccc3c2cccc3)O[Ni]21[N](c1c(cc(cc1Br)Br)Br)=Nc1c(ccc3c1cccc3)O2
• Title of publication: Crystal structures of a copper(II) and the isotypic nickel(II) and palladium(II) complexes of the ligand (<i>E</i>)-1-[(2,4,6-tribromophenyl)diazenyl]naphthalen-2-ol
• Authors of publication: Chetioui, Souheyla; Rouag, Djamil-Azzeddine; Djukic, Jean-Pierre; Bochet, Christian G.; Touzani, Rachid; Bailly, Corinne; Crochet, Aurélien; Fromm, Katharina M.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 8
• Pages of publication: 1093 - 1098
• a: 11.0909 ± 0.0006 Å
• b: 12.4571 ± 0.0006 Å
• c: 12.5382 ± 0.0007 Å
• α: 90°
• β: 107.82 ± 0.002°
• γ: 90°
• Cell volume: 1649.17 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0982
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.0797
• Weighted residual factors for all reflections included in the refinement: 0.0957
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes