Crystal structures of <i>fac</i>-tricarbonylchlorido(6,6'-dihydroxy-2,2'-bipyridine)rhenium(I) tetrahydrofuran monosolvate and <i>fac</i>-bromidotricarbonyl(6,6'-dihydroxy-2,2'-bipyridine)manganese(I) tetrahydrofuran monosolvate
Authors of publication
Lense, Sheri; Piro, Nicholas A.; Kassel, Scott W.; Wildish, Andrew; Jeffery, Brent
Journal of publication
Acta Crystallographica Section E
Year of publication
2016
Journal volume
72
Journal issue
8
Pages of publication
1201 - 1205
a
6.9661 ± 0.0006 Å
b
8.0082 ± 0.0006 Å
c
16.9007 ± 0.0013 Å
α
78.907 ± 0.002°
β
79.128 ± 0.002°
γ
88.886 ± 0.002°
Cell volume
908.46 ± 0.13 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
99.95 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.045
Residual factor for significantly intense reflections
0.033
Weighted residual factors for significantly intense reflections
0.0591
Weighted residual factors for all reflections included in the refinement
0.0628
Goodness-of-fit parameter for all reflections included in the refinement
