Information card for entry 2241870

Structure parameters

• Chemical name: [Bis(tetrahydrofuran)lithium]-di-μ-chlorido-{(<i>N</i>,<i>N</i>'-dicyclohexyl-1-butylamidinato-κ^2^<i>N</i>^1^,<i>N</i>^2^)[<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>'''-tetracyclohexyl-1-(1-butylamidinato)guanidinato-κ^2^<i>N</i>^1^,<i>N</i>^2^]holmate(III)}
• Formula: C55 H100 Cl2 Ho Li N6 O2
• Calculated formula: C55 H100 Cl2 Ho Li N6 O2
• Title of publication: Formation and structure of the first metal complexes comprising amidinoguanidinate ligands
• Authors of publication: Sroor, Farid M.; Liebing, Phil; Hrib, Cristian G.; Gräsing, Daniel; Hilfert, Liane; Edelmann, Frank T.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 11
• Pages of publication: 1526 - 1531
• a: 12.909 ± 0.003 Å
• b: 15.095 ± 0.003 Å
• c: 16.786 ± 0.003 Å
• α: 100.67 ± 0.03°
• β: 97.2 ± 0.03°
• γ: 109.5 ± 0.03°
• Cell volume: 2967.5 ± 1.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.0682
• Weighted residual factors for all reflections included in the refinement: 0.074
• Goodness-of-fit parameter for all reflections included in the refinement: 0.911
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes