Information card for entry 2241889

Structure parameters

• Chemical name: (<i>E</i>)-[Diazene-1,2-diylbis(4,1-phenylene)]bis(dimethylsilanol)
• Formula: C16 H22 N2 O2 Si2
• Calculated formula: C16 H22 N2 O2 Si2
• SMILES: c1(ccc(cc1)[Si](O)(C)C)/N=N/c1ccc(cc1)[Si](O)(C)C
• Title of publication: Crystal structures of 3,3'-bis(hydroxydimethylsilanyl)azobenzene and 4,4'-bis(hydroxydimethylsilane)azobenzene
• Authors of publication: Strüben, Jan; Hoffmann, Jonas; Presa-Soto, David; Näther, Christian; Staubitz, Anne
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 11
• Pages of publication: 1590 - 1594
• a: 17.8705 ± 0.0004 Å
• b: 10.0016 ± 0.0003 Å
• c: 20.5323 ± 0.0005 Å
• α: 90°
• β: 97.013 ± 0.002°
• γ: 90°
• Cell volume: 3642.36 ± 0.16 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0463
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes