Design of new anti-Alzheimer drugs: ring-expansion synthesis and synchrotron X-ray diffraction study of dimethyl 4-ethyl-11-fluoro-1,4,5,6,7,8-hexahydroazonino[5,6-<i>b</i>]indole-2,3-dicarboxylate
Authors of publication
Toze, Flavien A. A.; Listratova, Anna V.; Voskressensky, Leonid G.; Chernikova, Natalia Yu.; Lobanov, Nikolai N.; Bilyachenko, Alexey N.; Dorovatovskii, Pavel V.
Journal of publication
Acta Crystallographica Section E
Year of publication
2018
Journal volume
74
Journal issue
3
Pages of publication
298 - 301
a
8.4632 ± 0.0017 Å
b
10.993 ± 0.002 Å
c
20.52 ± 0.004 Å
α
90°
β
99.6 ± 0.03°
γ
90°
Cell volume
1882.4 ± 0.7 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1046
Residual factor for significantly intense reflections
0.0716
Weighted residual factors for significantly intense reflections
0.1625
Weighted residual factors for all reflections included in the refinement
0.1841
Goodness-of-fit parameter for all reflections included in the refinement
