Information card for entry 2242619

Structure parameters

• Chemical name: 3-(Triphenylphosphoranylidene)-2,5-dihydrofuran-2,5-dione tetrahydrofuran monosolvate
• Formula: C26 H25 O4 P
• Calculated formula: C26 H25 O4 P
• Title of publication: Crystal structure of 3-(triphenylphosphoranylidene)-2,5-dihydrofuran-2,5-dione tetrahydrofuran monosolvate
• Authors of publication: Zagidullin, Almaz; Islamov, Daut; Oshchepkova, Elena; Lonnecke, Peter; Miluykov, Vasili
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2018
• Journal volume: 74
• Journal issue: 9
• Pages of publication: 1336 - 1338
• a: 12.1287 ± 0.0005 Å
• b: 10.553 ± 0.0004 Å
• c: 17.5838 ± 0.0008 Å
• α: 90°
• β: 104.435 ± 0.004°
• γ: 90°
• Cell volume: 2179.57 ± 0.16 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0995
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1145
• Weighted residual factors for all reflections included in the refinement: 0.1301
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes