Crystal structures of two nickel(II) macrocyclic salts: (5,7,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) bis(perchlorate) monohydrate and (5,7,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) dibromide trihydrate
Authors of publication
Corfield, Peter W. R.; Goedken, Virgil L.
Journal of publication
Acta Crystallographica Section E
Year of publication
2019
Journal volume
75
Journal issue
3
Pages of publication
332 - 337
a
8.906 ± 0.004 Å
b
29.412 ± 0.011 Å
c
19.505 ± 0.009 Å
α
90°
β
107.03 ± 0.019°
γ
90°
Cell volume
4885 ± 4 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0737
Residual factor for significantly intense reflections
0.04341
Weighted residual factors for significantly intense reflections
0.0992
Weighted residual factors for all reflections included in the refinement
0.1092
Goodness-of-fit parameter for all reflections included in the refinement
