Information card for entry 2242860

Structure parameters

• Chemical name: 1,3-Di-<i>tert</i>-butyl-2-chloro-4,4-diphenyl-1,3,2λ^3^,4-\ diazaphosphasiletidine
• Formula: C20 H28 Cl N2 P Si
• Calculated formula: C20 H28 Cl N2 P Si
• Title of publication: Synthesis and crystal structure of 1,3-di-<i>tert</i>-butyl-2-chloro-4,4-diphenyl-1,3,2λ^3^,4-diazaphosphasiletidine
• Authors of publication: Mo, Dennis; Frank, Walter
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2019
• Journal volume: 75
• Journal issue: 3
• Pages of publication: 405 - 409
• a: 13.4004 ± 0.0007 Å
• b: 15.6272 ± 0.0006 Å
• c: 10.3817 ± 0.0005 Å
• α: 90°
• β: 95.739 ± 0.004°
• γ: 90°
• Cell volume: 2163.14 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0799
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.098
• Weighted residual factors for all reflections included in the refinement: 0.1038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.495
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes