Absolute structure of (3a<i>S</i>,5<i>S</i>,7a<i>S</i>,7b<i>S</i>,9a<i>R</i>,10<i>R</i>,12a<i>R</i>,12b<i>S</i>)-7b-hydroxy-4,4,7a,9a,12a-pentamethyl-10-[(2'<i>R</i>)-6-methylheptan-2-yl]-2,8,9-trioxooctadecahydrobenzo[<i>d</i>]indeno[4,5-<i>b</i>]azepin-5-yl acetate from 62-year-old crystals
Authors of publication
Suescun, Leopoldo; Heinzen, Horacio
Journal of publication
Acta Crystallographica Section E
Year of publication
2019
Journal volume
75
Journal issue
9
Pages of publication
1348 - 1351
a
34.882 ± 0.004 Å
b
6.5332 ± 0.0011 Å
c
13.6021 ± 0.0016 Å
α
90°
β
100.599 ± 0.014°
γ
90°
Cell volume
3046.9 ± 0.7 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
5
Hermann-Mauguin space group symbol
C 1 2 1
Hall space group symbol
C 2y
Residual factor for all reflections
0.0549
Residual factor for significantly intense reflections
0.0504
Weighted residual factors for significantly intense reflections
0.1306
Weighted residual factors for all reflections included in the refinement
0.1346
Goodness-of-fit parameter for all reflections included in the refinement
