Information card for entry 2243610

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[bis(3-oxo-1,3-diphenylprop-1-enolato-κ^2^<i>O</i>,<i>O</i>')zinc(II)]-μ~2~-tris[4-(pyridin-3-yl)phenyl]amine-κ^2^<i>N</i>:<i>N</i>'] tetrahydrofuran monosolvate]
• Formula: C67 H54 N4 O5 Zn
• Calculated formula: C67 H54 N4 O5 Zn
• Title of publication: Crystal structure of <i>catena</i>-poly[[[bis(3-oxo-1,3-diphenylprop-1-enolato-κ^2^<i>O</i>,<i>O</i>')zinc(II)]-μ~2~-tris[4-(pyridin-3-yl)phenyl]amine-κ^2^<i>N</i>:<i>N</i>'] tetrahydrofuran monosolvate]
• Authors of publication: Kashiwagi, Yukiyasu; Kubono, Koji; Tamai, Toshiyuki
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2019
• Journal volume: 75
• Journal issue: 10
• Pages of publication: 1432 - 1435
• a: 27.2823 ± 0.0014 Å
• b: 19.7693 ± 0.0012 Å
• c: 9.9674 ± 0.0005 Å
• α: 90°
• β: 94.614 ± 0.007°
• γ: 90°
• Cell volume: 5358.5 ± 0.5 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0959
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1152
• Weighted residual factors for all reflections included in the refinement: 0.1284
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes