Information card for entry 2243843

Structure parameters

• Chemical name: Tetrakis[μ~2~-1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-olato]tetrakis(μ~3~-2-methylpropan-2-olato)octacopper(I)
• Formula: C32 H36 Cu8 F36 O8
• Calculated formula: C32 H36 Cu8 F36 O8
• Title of publication: Tetrakis[μ~2~-1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)propan-2-olato]tetrakis(μ~3~-2-methylpropan-2-olato)octacopper(I)
• Authors of publication: Purdy, Andrew P.; Butcher, Ray J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2021
• Journal volume: 77
• Journal issue: 6
• Pages of publication: 668 - 671
• a: 10.3302 ± 0.0002 Å
• b: 19.5926 ± 0.0005 Å
• c: 13.1516 ± 0.0003 Å
• α: 90°
• β: 101.004 ± 0.001°
• γ: 90°
• Cell volume: 2612.88 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0609
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1027
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes