Crystal structures of the sulfones of 2,3-diphenyl-2,3-di-hydro-4<i>H</i>-1,3-benzo-thia-zin-4-one and 2,3-diphenyl-2,3-di-hydro-4<i>H</i>-pyrido[3,2-<i>e</i>][1,3]thia-zin-4-one.
Authors of publication
Yennawar, Hemant P.; Mal, Tapas K.; Pacheco, Carlos N.; Lagalante, Anthony F.; Olsen, Mark A.; Russell, Michael W.; Muench, Grace C.; Moyer, Quentin J.; Silverberg, Lee J.
Journal of publication
Acta crystallographica. Section E, Crystallographic communications
Year of publication
2023
Journal volume
79
Journal issue
Pt 3
Pages of publication
221 - 225
a
6.8584 ± 0.0019 Å
b
25.487 ± 0.007 Å
c
19.008 ± 0.005 Å
α
90°
β
94.669 ± 0.007°
γ
90°
Cell volume
3311.6 ± 1.6 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0773
Residual factor for significantly intense reflections
0.051
Weighted residual factors for significantly intense reflections
0.1226
Weighted residual factors for all reflections included in the refinement
0.1382
Goodness-of-fit parameter for all reflections included in the refinement
