Information card for entry 2312140

Structure parameters

• Formula: Ag2.8 Cu0.2 Pb9.77 S28 Sb11.23
• Calculated formula: Ag2.803 Cu0.198 Pb9.772 S28 Sb11.228
• Title of publication: A fresh view on the structure and twinning of owyheeite, a rod-polytype and twofold superstructure.
• Authors of publication: Stöger, Berthold; Göb, Christian; Topa, Dan
• Journal of publication: Acta crystallographica Section B, Structural science, crystal engineering and materials
• Year of publication: 2023
• Journal volume: 79
• Journal issue: 4
• a: 8.1882 ± 0.0003 Å
• b: 27.2641 ± 0.0007 Å
• c: 22.8679 ± 0.0007 Å
• α: 90°
• β: 90.283 ± 0.003°
• γ: 90°
• Cell volume: 5105.1 ± 0.3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0655
• Weighted residual factors for significantly intense reflections: 0.1324
• Weighted residual factors for all reflections included in the refinement: 0.1464
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes