Information card for entry 2312505

Structure parameters

• Chemical name: Bis(4'-phenyl-2,2':6',2''-terpyridine)nickel(II) bis(perchlorate)
• Formula: C42 H30 Cl2 N6 Ni O8
• Calculated formula: C42 H30 Cl2 N6 Ni O8
• Title of publication: Synthesis, characterization and structural analysis of complexes from 2,2':6',2''-terpyridine derivatives with transition metals.
• Authors of publication: Fajardo, Daniel A.; Arteaga, Danny; Ellena, Javier; Santiago, Pedro H. O.; D'Vries, Richard F; Lenis, Luis Alberto
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2024
• Journal volume: 80
• Journal issue: 6
• a: 9.3581 ± 0.0002 Å
• b: 12.6255 ± 0.0003 Å
• c: 31.4046 ± 0.0008 Å
• α: 90°
• β: 97.038 ± 0.002°
• γ: 90°
• Cell volume: 3682.52 ± 0.15 ų
• Cell temperature: 99.99 ± 0.14 K
• Ambient diffraction temperature: 99.99 ± 0.14 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0844
• Weighted residual factors for all reflections included in the refinement: 0.0937
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes