Information card for entry 2312845

Structure parameters

• Chemical name: (μ~2~-3,6-Diphenylnemzene-1,2,4,5-tetraolato)bis[{tris[(pyridin-2-yl)methyl]amine}gallium(II)] bis(tetraphenylborate) dimethylformamide tetrasolvate
• Formula: C114 H114 B2 Ga2 N12 O8
• Calculated formula: C114 H114 B2 Ga2 N12 O8
• Title of publication: Synthesis and crystal structures of a family of bimetallic complexes with phenyl-substituted bridging tetraoxolene ligands.
• Authors of publication: Kamin, Ashlyn A.; Le, Phuong H.; Brannan, E. J.; Gannon, Paige M.; Krajewski, Sebastian; Kaminsky, Werner; Xiao, Dianne J.
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2025
• Journal volume: 81
• Journal issue: 6
• a: 11.4707 ± 0.0012 Å
• b: 12.3775 ± 0.0012 Å
• c: 18.1357 ± 0.0019 Å
• α: 90.729 ± 0.005°
• β: 103.969 ± 0.005°
• γ: 103.874 ± 0.004°
• Cell volume: 2419 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0998
• Weighted residual factors for all reflections included in the refinement: 0.1045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes