Information card for entry 2312870

Structure parameters

• Chemical name: Carbonyl(4,4'-di-<i>tert</i>-butyl-2,2'-bypyridine)hydridobis(triphenylphosphane)ruthenium(II) hexaflurophosphate
• Formula: C55 H55 F6 N2 O P3 Ru
• Calculated formula: C55 H55 F6 N2 O P3 Ru
• Title of publication: Synthesis and structural characterization of ruthenium(II) hydrido carbonyl triphenylphosphine α-diimine complexes with derivatives of 2,2'-bipyridine.
• Authors of publication: Wysocki, Waldemar; Karczmarzyk, Zbigniew; Kamecka, Anna
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2025
• Journal volume: 81
• Journal issue: 7
• a: 29.96 ± 0.002 Å
• b: 11.7394 ± 0.0005 Å
• c: 31.263 ± 0.002 Å
• α: 90°
• β: 109.849 ± 0.008°
• γ: 90°
• Cell volume: 10342.3 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/c 1
• Hall space group symbol: -I 2yc
• Residual factor for all reflections: 0.1362
• Residual factor for significantly intense reflections: 0.0835
• Weighted residual factors for significantly intense reflections: 0.1976
• Weighted residual factors for all reflections included in the refinement: 0.2338
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes