Synthesis and Electropolymerization of Hexadecyl Functionalized Bithiophene and Thieno[3,2-b]thiophene End-Capped with EDOT and EDTT Units
Authors of publication
McEntee, Greg J.; Skabara, Peter J.; Vilela, Filipe; Tierney, Steven; Samuel, Ifor D. W.; Gambino, Salvatore; Coles, Simon J.; Hursthouse, Michael B.; Harrington, Ross W.; Clegg, William
Journal of publication
Chemistry of Materials
Year of publication
2010
Journal volume
22
Journal issue
9
Pages of publication
3000
a
7.1255 ± 0.0001 Å
b
11.4922 ± 0.0002 Å
c
16.5104 ± 0.0003 Å
α
71.958 ± 0.001°
β
83.543 ± 0.001°
γ
82.168 ± 0.001°
Cell volume
1269.98 ± 0.04 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
3
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0542
Residual factor for significantly intense reflections
0.0431
Weighted residual factors for significantly intense reflections
0.0868
Weighted residual factors for all reflections included in the refinement
0.0932
Goodness-of-fit parameter for all reflections included in the refinement
