Information card for entry 4023967

Structure parameters

• Common name: Fraenkel 1469
• Formula: C32 H58 Li2 N2
• Calculated formula: C32 H58 Li2 N2
• Title of publication: Structural Distortions and Dynamic Behavior of the Elusive "L"-Shaped cis-Bicyclo[3.3.0]octenyllithium: X-ray Crystallographic and NMR Studies
• Authors of publication: Gideon Fraenkel; Xiao Chen; Judith Gallucci; Yan Lu
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2007
• Journal volume: 72
• Pages of publication: 4961 - 4965
• a: 11.3719 ± 0.001 Å
• b: 17.364 ± 0.002 Å
• c: 16.532 ± 0.003 Å
• α: 90°
• β: 99.11 ± 0.005°
• γ: 90°
• Cell volume: 3223.4 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1396
• Weighted residual factors for all reflections included in the refinement: 0.1471
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No