Information card for entry 4027892

Structure parameters

• Formula: C19 H33 N O3.1 Si
• Calculated formula: C19 H33 N O3.098 Si
• SMILES: [Si](O[C@H]1[C@H](CC(=O)[C@H]2[C@@H]3N(CCC3)C(=O)C[C@H]12)C)(C)(C)C(C)(C)C
• Title of publication: Total Synthesis of the Lycopodium Alkaloid Serratezomine A Using Free Radical-Mediated Vinyl Amination to Prepare a β-Stannyl Enamine Linchpin
• Authors of publication: Julie A. Pigza; Jeong-Seok Han; Aroop Chandra; Daniel Mutnick; Maren Pink; Jeffrey N. Johnston
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2013
• Journal volume: 78
• Pages of publication: 822 - 843
• a: 24.705 ± 0.009 Å
• b: 6.725 ± 0.003 Å
• c: 11.915 ± 0.004 Å
• α: 90°
• β: 97.458 ± 0.009°
• γ: 90°
• Cell volume: 1962.8 ± 1.3 ų
• Cell temperature: 117 ± 2 K
• Ambient diffraction temperature: 117 ± 2 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.0845
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No