Crystallography Open Database

Information card for entry 4028369

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Structure parameters

Formula	C30 H37.36 N O6.18
Calculated formula	C30 H37.36 N O6.18
Title of publication	Diastereoselective Synthesis of Tetrahydrofurans by Lewis Acid Catalyzed Intermolecular Carbenoid-Carbonyl Reaction-Cycloaddition Sequences: Unusual Diastereoselectivity of Lewis Acid Catalyzed Cycloadditions
Authors of publication	Yuta Hashimoto; Kennosuke Itoh; Akikazu Kakehi; Motoo Shiro; Hiroyuki Suga
Journal of publication	Journal of Organic Chemistry
Year of publication	2013
Journal volume	78
Pages of publication	6182 - 6195
a	14.9082 ± 0.0003 Å
b	18.0949 ± 0.0003 Å
c	20.7986 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	5610.7 ± 0.4 Å³
Cell temperature	153.1 K
Ambient diffraction temperature	153.1 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for significantly intense reflections	0.0619
Weighted residual factors for all reflections included in the refinement	0.1601
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	1.54187 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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