Information card for entry 4031999

Structure parameters

• Formula: C23 H26 F2 N2 O2
• Calculated formula: C23 H26 F2 N2 O2
• SMILES: FC(F)(CC1(C(=O)N(c2c1cccc2)C)Cc1ccccc1)C(=O)N(CC)CC
• Title of publication: Silver-Catalyzed Difluoroamidation of Activated Alkenes for the Construction of Difluorinated 3,3-Disubstituted Oxindoles.
• Authors of publication: Wang, Chao; Chen, Qiao; Guo, Quanping; Liu, Hong; Xu, Zhaoqing; Liu, Yubing; Wang, Mengran; Wang, Rui
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2016
• Journal volume: 81
• Journal issue: 13
• Pages of publication: 5782 - 5788
• a: 14.3541 ± 0.0008 Å
• b: 12.9841 ± 0.0009 Å
• c: 23.2417 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4331.7 ± 0.5 ų
• Cell temperature: 295.06 ± 0.1 K
• Ambient diffraction temperature: 295.06 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.2101
• Residual factor for significantly intense reflections: 0.0951
• Weighted residual factors for significantly intense reflections: 0.2415
• Weighted residual factors for all reflections included in the refinement: 0.3318
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No