A Palladium-Catalyzed Ullmann Cross-Coupling/Reductive Cyclization Route to the Carbazole Natural Products 3-Methyl-9H-carbazole, Glycoborine, Glycozoline, Clauszoline K, Mukonine, and Karapinchamine A.
Authors of publication
Yan, Qiao; Gin, Emma; Wasinska-Kalwa, Malgorzata; Banwell, Martin G.; Carr, Paul D.
Journal of publication
The Journal of organic chemistry
Year of publication
2017
Journal volume
82
Journal issue
8
Pages of publication
4148 - 4159
a
15.7767 ± 0.0002 Å
b
9.4629 ± 0.0001 Å
c
16.1402 ± 0.0002 Å
α
90°
β
91.7342 ± 0.0013°
γ
90°
Cell volume
2408.52 ± 0.05 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0466
Residual factor for significantly intense reflections
0.0389
Weighted residual factors for all reflections
0.0767
Weighted residual factors for significantly intense reflections
0.0687
Weighted residual factors for all reflections included in the refinement
0.0767
Goodness-of-fit parameter for all reflections included in the refinement
