Reactions of 3,3,3-Trihalogeno-1-nitropropenes with Arenes in the Superacid CF<sub>3</sub>SO<sub>3</sub>H: Synthesis of ( Z)-3,3,3-Trihalogeno-1,2-diarylpropan-1-one Oximes and Study on the Reaction Mechanism.
Authors of publication
Golushko, Andrei A.; Sandzhieva, Maria A.; Ivanov, Alexander Yu; Boyarskaya, Irina A.; Khoroshilova, Olesya V.; Barkov, Alexey Yu; Vasilyev, Aleksander V.
Journal of publication
The Journal of organic chemistry
Year of publication
2018
Journal volume
83
Journal issue
17
Pages of publication
10142 - 10157
a
6.4856 ± 0.0005 Å
b
10.5126 ± 0.0011 Å
c
13.3256 ± 0.0013 Å
α
104.204 ± 0.009°
β
93.568 ± 0.007°
γ
97.731 ± 0.007°
Cell volume
868.46 ± 0.15 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1517
Residual factor for significantly intense reflections
0.0976
Weighted residual factors for significantly intense reflections
0.2832
Weighted residual factors for all reflections included in the refinement
0.3317
Goodness-of-fit parameter for all reflections included in the refinement
