Reactions of 3,3,3-Trihalogeno-1-nitropropenes with Arenes in the Superacid CF<sub>3</sub>SO<sub>3</sub>H: Synthesis of ( Z)-3,3,3-Trihalogeno-1,2-diarylpropan-1-one Oximes and Study on the Reaction Mechanism.
Authors of publication
Golushko, Andrei A.; Sandzhieva, Maria A.; Ivanov, Alexander Yu; Boyarskaya, Irina A.; Khoroshilova, Olesya V.; Barkov, Alexey Yu; Vasilyev, Aleksander V.
Journal of publication
The Journal of organic chemistry
Year of publication
2018
Journal volume
83
Journal issue
17
Pages of publication
10142 - 10157
a
5.8087 ± 0.0003 Å
b
15.6067 ± 0.0008 Å
c
16.7214 ± 0.0008 Å
α
90°
β
90°
γ
90°
Cell volume
1515.87 ± 0.13 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0378
Residual factor for significantly intense reflections
0.0373
Weighted residual factors for significantly intense reflections
0.1052
Weighted residual factors for all reflections included in the refinement
0.1058
Goodness-of-fit parameter for all reflections included in the refinement
