Diastereoselective Ammonium-Directed Epoxidation in the Asymmetric Syntheses of Dihydroconduramines (+)-C-2, (-)-C-2, (+)-D-2, (+)-E-2, (+)-F-2, and (-)-F-2.
Authors of publication
Da Silva Pinto, Solange; Davies, Stephen G.; Fletcher, Ai M.; Roberts, Paul M.; Thomson, James E.
Journal of publication
The Journal of organic chemistry
Year of publication
2018
Journal volume
83
Journal issue
17
Pages of publication
9939 - 9957
a
5.71465 ± 0.00009 Å
b
11.1475 ± 0.0002 Å
c
9.58011 ± 0.00015 Å
α
90°
β
106.521 ± 0.0017°
γ
90°
Cell volume
585.097 ± 0.017 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0274
Residual factor for significantly intense reflections
0.0267
Weighted residual factors for all reflections
0.0663
Weighted residual factors for significantly intense reflections
0.0657
Weighted residual factors for all reflections included in the refinement
0.0663
Goodness-of-fit parameter for all reflections included in the refinement
