Crystallography Open Database

Information card for entry 4035365

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Coordinates	4035365.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H30 N O4
Calculated formula	C24 H30 N O4
Title of publication	From CO<sub>2</sub> to 4 H-Quinolizin-4-ones: A One-Pot Multicomponent Approach via Ag<sub>2</sub>O/Cs<sub>2</sub>CO<sub>3</sub> Orthogonal Tandem Catalysis.
Authors of publication	Dong, Chao-Chen; Xiang, Jun-Feng; Xu, Li-Jin; Gong, Han-Yuan
Journal of publication	The Journal of organic chemistry
Year of publication	2018
Journal volume	83
Journal issue	16
Pages of publication	9561 - 9567
a	8.7892 ± 0.0018 Å
b	9.969 ± 0.002 Å
c	13.277 ± 0.003 Å
α	86.63 ± 0.03°
β	73.04 ± 0.03°
γ	82.14 ± 0.03°
Cell volume	1102.1 ± 0.4 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0866
Residual factor for significantly intense reflections	0.0802
Weighted residual factors for significantly intense reflections	0.1852
Weighted residual factors for all reflections included in the refinement	0.1922
Goodness-of-fit parameter for all reflections included in the refinement	1.003
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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