Total Syntheses of the 3H-Pyrrolo[2,3-c]quinolone-containing Alkaloids Marinoquinolines A-F, K and Aplidiopsamine A Using a Palladium-catalysed Ullmann Cross-coupling/Reductive Cyclization Pathway.
Authors of publication
Bolte, Benoit; Bryan, Christopher S.; Sharp, Phillip P.; Sayyahi, Soheil; Rihouey, Charly; Kendrick, Amy; Lan, Ping; Banwell, Martin G.; Jackson, Colin J.; Fraser, Nicholas J.; Willis, Anthony C.; Ward, James S.
Journal of publication
The Journal of organic chemistry
Year of publication
2019
a
13.4569 ± 0.0002 Å
b
6.5269 ± 0.0001 Å
c
17.6639 ± 0.0002 Å
α
90°
β
109.247 ± 0.0016°
γ
90°
Cell volume
1464.73 ± 0.04 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0345
Residual factor for significantly intense reflections
0.0321
Weighted residual factors for all reflections
0.0812
Weighted residual factors for significantly intense reflections
0.0794
Weighted residual factors for all reflections included in the refinement
0.0812
Goodness-of-fit parameter for all reflections included in the refinement
