Identification of the Side Products That Diminish the Yields of the Monoamidated Product in Metal-Catalyzed C–H Amidation of 2-Phenylpyridine with Arylisocyanates
Authors of publication
McKay, Alasdair I.; Altalhi, Weam A. O.; McInnes, Lachlan E.; Czyz, Milena L.; Canty, Allan J.; Donnelly, Paul S.; O’Hair, Richard A. J.
Journal of publication
The Journal of Organic Chemistry
Year of publication
2020
a
7.7093 ± 0.0005 Å
b
9.5441 ± 0.0005 Å
c
12.4195 ± 0.0004 Å
α
94.235 ± 0.003°
β
93.075 ± 0.004°
γ
113.306 ± 0.005°
Cell volume
833.52 ± 0.08 Å3
Cell temperature
100 ± 0.1 K
Ambient diffraction temperature
100 ± 0.1 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0501
Residual factor for significantly intense reflections
0.0465
Weighted residual factors for significantly intense reflections
0.1284
Weighted residual factors for all reflections included in the refinement
0.1308
Goodness-of-fit parameter for all reflections included in the refinement
