A covalent and modular synthesis of homo and hetero [n]rotaxanes.
Authors of publication
Cornelissen, Milo D.; Pilon, Simone; Steemers, Luuk; Wanner, Martin J.; Frölke, Steven; Zuidinga, Ed; Jorgensen, Steen Ingemann; van der Vlugt, Jarl Ivar; van Maarseveen, Jan H.
Journal of publication
The Journal of organic chemistry
Year of publication
2020
a
8.7409 ± 0.0019 Å
b
12.748 ± 0.003 Å
c
13.057 ± 0.003 Å
α
105.542 ± 0.006°
β
94.855 ± 0.006°
γ
96.174 ± 0.006°
Cell volume
1383.8 ± 0.5 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1835
Residual factor for significantly intense reflections
0.1547
Weighted residual factors for significantly intense reflections
0.3741
Weighted residual factors for all reflections included in the refinement
0.4082
Goodness-of-fit parameter for all reflections included in the refinement
