Synthesis of <i>N</i><i> <sub>β</sub> </i>-Substituted α,β-Diamino Acids via Stereoselective <i>N</i>-Michael Additions to a Chiral Bicyclic Dehydroalanine.
Authors of publication
Navo, Claudio D.; Mazo, Nuria; Oroz, Paula; Gutiérrez-Jiménez, Marta I; Marín, Javier; Asenjo, Juan; Avenoza, Alberto; Busto, Jesús H; Corzana, Francisco; Zurbano, María M; Jiménez-Osés, Gonzalo; Peregrina, Jesús M
Journal of publication
The Journal of organic chemistry
Year of publication
2020
a
12.0249 ± 0.0011 Å
b
7.4099 ± 0.0006 Å
c
13.555 ± 0.0012 Å
α
90°
β
113.483 ± 0.003°
γ
90°
Cell volume
1107.76 ± 0.17 Å3
Cell temperature
110 ± 2 K
Ambient diffraction temperature
110 ± 2 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0522
Residual factor for significantly intense reflections
0.0389
Weighted residual factors for significantly intense reflections
0.1007
Weighted residual factors for all reflections included in the refinement
0.1055
Goodness-of-fit parameter for all reflections included in the refinement
