Information card for entry 4038663

Structure parameters

• Formula: C26 H56 F6 P Sb Si4
• Calculated formula: C26 H56 F6 P Sb Si4
• Title of publication: Trialkylphosphines Having a Bulky Phosphacyclopentane Backbone: Structural and Redox Properties Depending on the Exocyclic Alkyl Groups and EPR Observation of a Persistent Trialkylphosphine Radical Cation.
• Authors of publication: Hirakawa, Fumiya; Nakagawa, Hiroshi; Honda, Shunya; Ishida, Shintaro; Iwamoto, Takeaki
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 11.3052 ± 0.0004 Å
• b: 16.6951 ± 0.0006 Å
• c: 17.9915 ± 0.0006 Å
• α: 90°
• β: 90.973 ± 0.001°
• γ: 90°
• Cell volume: 3395.3 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0238
• Residual factor for significantly intense reflections: 0.0208
• Weighted residual factors for significantly intense reflections: 0.0501
• Weighted residual factors for all reflections included in the refinement: 0.0524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No