Information card for entry 4038724

Structure parameters

• Formula: C23 H29 F O7
• Calculated formula: C23 H29 F O7
• Title of publication: Palladium-Catalyzed ortho-C-H Glycosylation/ipso-Alkenylation of Aryl Iodides.
• Authors of publication: Ding, Ya-Nan; Shi, Wei-Yu; Liu, Ce; Zheng, Nian; Li, Ming; An, Yang; Zhang, Zhe; Wang, Cui-Tian; Zhang, Bo-Sheng; Liang, Yong-Min
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2020
• a: 15.424 ± 0.0005 Å
• b: 9.5366 ± 0.00019 Å
• c: 17.1423 ± 0.0005 Å
• α: 90°
• β: 115.321 ± 0.004°
• γ: 90°
• Cell volume: 2279.25 ± 0.13 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1215
• Weighted residual factors for all reflections included in the refinement: 0.1261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No