Collective Syntheses of Guaiane Sesquiterpenes: Stereoselective Syntheses of (+)-Dysodensiol F, (+)-10β,14-Dihydroxy-<i>allo</i>-aromadendrane, and (-)-Dendroside C Aglycon.
Authors of publication
Kim, Hyun Su; Park, Hyunkyung; Lim, Juhee; Lim, Changjin; Kim, Taewoo; Lee, Seungbeom; Hur, Joonseong; Sim, Jaehoon; Choi, Hyun Jin; Suh, Young-Ger
Journal of publication
The Journal of organic chemistry
Year of publication
2020
a
8.3608 ± 0.0001 Å
b
16.9291 ± 0.0001 Å
c
23.1401 ± 0.0002 Å
α
90°
β
90°
γ
90°
Cell volume
3275.27 ± 0.05 Å3
Cell temperature
99.9 ± 0.4 K
Ambient diffraction temperature
99.9 ± 0.4 K
Number of distinct elements
5
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0287
Residual factor for significantly intense reflections
0.0276
Weighted residual factors for significantly intense reflections
0.0721
Weighted residual factors for all reflections included in the refinement
0.073
Goodness-of-fit parameter for all reflections included in the refinement