Information card for entry 4038956

Structure parameters

• Formula: C16 H36 N14 O26 Sm2
• Calculated formula: C16 H36 N14 O26 Sm2
• Title of publication: New binuclear bis(2,4,6,8-tetramethyl-2,4,6,8-tetraazobicyclo(3.3.0)octane-3,7-dione-O,O')-tetraaqua-hexakis(nitrato-O,O')-disamarium(III) complex: Synthesis and crystal structure
• Authors of publication: Netreba, E.E.; Sarnit, E.A.; Shabanov, S.V.; Velikozhon, A.A.
• Journal of publication: Russian Journal of Inorganic Chemistry
• Year of publication: 2017
• Journal volume: 62
• Journal issue: 5
• Pages of publication: 654 - 658
• a: 9.8661 ± 0.0002 Å
• b: 10.2913 ± 0.0003 Å
• c: 10.9629 ± 0.0003 Å
• α: 74.475 ± 0.002°
• β: 67.802 ± 0.002°
• γ: 67.57 ± 0.002°
• Cell volume: 942.68 ± 0.05 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0155
• Residual factor for significantly intense reflections: 0.0146
• Weighted residual factors for significantly intense reflections: 0.0378
• Weighted residual factors for all reflections included in the refinement: 0.0381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No