Information card for entry 4060083

Structure parameters

• Chemical name: (pentamethylcyclopentadienyl)(triisopropylmethylphosphine) (trihydrosilyl)ruthenium dihydride
• Formula: C19 H41 P Ru Si
• Calculated formula: C19 H41 P Ru Si
• Title of publication: Syntheses and X-ray Diffraction Studies of Half-Sandwich Hydridosilyl Complexes of Ruthenium
• Authors of publication: Osipov, Alexander L.; Gerdov, Sergei M.; Kuz'mina, Lyudmila G.; Howard, Judith A. K.; Nikonov, Georgii I.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 4
• Pages of publication: 587 - 602
• a: 33.0396 ± 0.0013 Å
• b: 8.9192 ± 0.0004 Å
• c: 14.8864 ± 0.0006 Å
• α: 90°
• β: 101.646 ± 0.001°
• γ: 90°
• Cell volume: 4296.5 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0284
• Weighted residual factors for significantly intense reflections: 0.0673
• Weighted residual factors for all reflections included in the refinement: 0.0718
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No