Information card for entry 4060091

Structure parameters

• Formula: C104 H97 As4 Co4 F12 N4 O40.5 Pt2 S4
• Calculated formula: C104 H80 As4 Co4 F12 N4 O40.5 Pt2 S4
• Title of publication: Cationic M(II)/Co(0) (M = Pd, Pt) Metallomacrocycles Containing Tetrahedral Co~2~C~24 Cluster Cores Formed by Self-Assembly of Cluster-Bridged Bipyridine (4-C~5~H~4~NCO~2~CH~2~)~2~C~2~Co~2~(CO)~6~ and Diarsine-Chelated Complex [Pd(dpab)(H~2~O)(OTf)][OTf] or [Pt(dpab)(H~2~O)~2~][OTf]~2~
• Authors of publication: Li-Cheng Song; Guo-Xia Jin; Wen-Xiong Zhang; Qing-Mei Hu
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Pages of publication: 700 - 706
• a: 13.667 ± 0.009 Å
• b: 17.272 ± 0.011 Å
• c: 18.06 ± 0.012 Å
• α: 92.019 ± 0.012°
• β: 101.885 ± 0.011°
• γ: 104.029 ± 0.011°
• Cell volume: 4031 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1399
• Residual factor for significantly intense reflections: 0.0689
• Weighted residual factors for significantly intense reflections: 0.2004
• Weighted residual factors for all reflections included in the refinement: 0.2398
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No