Information card for entry 4063208

Structure parameters

• Formula: C34 H29 O4 Rh
• Calculated formula: C34 H29 O4 Rh
• Title of publication: Rhodium Acetylacetonate and Iron Tricarbonyl Complexes of Tetracyclone and 3-Ferrocenyl-2,4,5-triphenylcyclopentadienone: An X-ray Crystallographic and NMR Study
• Authors of publication: Hari K. Gupta; Nicole Rampersad; Mark Stradiotto; Michael J. McGlinchey
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Pages of publication: 184 - 191
• a: 8.823 ± 0.003 Å
• b: 12.404 ± 0.004 Å
• c: 15.694 ± 0.005 Å
• α: 66.929 ± 0.007°
• β: 81.291 ± 0.008°
• γ: 73.873 ± 0.006°
• Cell volume: 1516.2 ± 0.8 ų
• Cell temperature: 299 ± 2 K
• Ambient diffraction temperature: 299 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.133
• Residual factor for significantly intense reflections: 0.1161
• Weighted residual factors for all reflections: 0.3462
• Weighted residual factors for significantly intense reflections: 0.3339
• Goodness-of-fit parameter for all reflections: 1.52
• Goodness-of-fit parameter for significantly intense reflections: 1.653
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No