Information card for entry 4063696

Structure parameters

• Formula: C90 H110 Br4 N8 Pd2
• Calculated formula: C90 H110 Br4 N8 Pd2
• Title of publication: Synthesis and Structure of Dinuclear Silver(I) and Palladium(II) Complexes of 2,7-Bis(methylene)naphthalene-Bridged Bis-N-Heterocyclic Carbene Ligands
• Authors of publication: Saito, Shinichi; Saika, Mitsuya; Yamasaki, Ryu; Azumaya, Isao; Masu, Hyuma
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 6
• Pages of publication: 1366
• a: 21.009 ± 0.005 Å
• b: 17.498 ± 0.004 Å
• c: 25.748 ± 0.006 Å
• α: 90°
• β: 96.463 ± 0.004°
• γ: 90°
• Cell volume: 9405 ± 4 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1312
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1498
• Weighted residual factors for all reflections included in the refinement: 0.171
• Goodness-of-fit parameter for all reflections included in the refinement: 0.855
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No