Information card for entry 4063735

Structure parameters

• Formula: C36 H40 B Mo N6 O3 Sn
• Calculated formula: C36 H40 B Mo N6 O3 Sn
• Title of publication: Group 14 Substituted Carbyne Complexes—An Almost Complete Set: [Mo(\τb CAPh3)(CO)2(Tp*)] (Tp* = Hydrotris(dimethylpyrazolyl)borate; A = Si, Ge, Sn, Pb but A ≠ C)
• Authors of publication: Cordiner, Richard L.; Hill, Anthony F.; Shang, Rong; Willis, Anthony C.
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 1
• Pages of publication: 139
• a: 8.0951 ± 0.0003 Å
• b: 9.969 ± 0.0005 Å
• c: 23.1787 ± 0.0011 Å
• α: 82.3925 ± 0.0018°
• β: 88.749 ± 0.002°
• γ: 77.05 ± 0.002°
• Cell volume: 1806.84 ± 0.14 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1191
• Residual factor for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections: 0.0796
• Weighted residual factors for significantly intense reflections: 0.066
• Weighted residual factors for all reflections included in the refinement: 0.066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.145
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No