Information card for entry 4064373

Structure parameters

• Chemical name: Lithium[2-(1,3-bis-(2',6'-dimethylphenyl)[1,3,2]diazaphospholenyl-3- diphenylphosphino-1-cyanoethanide]dichloropalladium(II)
• Formula: C41 H45 Cl2 Li N6 P2 Pd
• Calculated formula: C41 H45 Cl2 Li N6 P2 Pd
• Title of publication: Synthesis and Characterization of an Unsymmetrical 1,2-Diphosphinoethanide Complex
• Authors of publication: Förster, Daniela; Nieger, Martin; Gudat, Dietrich
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 9
• Pages of publication: 2628
• a: 10.471 ± 0.001 Å
• b: 14.436 ± 0.001 Å
• c: 15.933 ± 0.002 Å
• α: 107.57 ± 0.01°
• β: 102.66 ± 0.01°
• γ: 109.74 ± 0.01°
• Cell volume: 2018 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1169
• Residual factor for significantly intense reflections: 0.0696
• Weighted residual factors for significantly intense reflections: 0.1637
• Weighted residual factors for all reflections included in the refinement: 0.1911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No