Information card for entry 4065525

Structure parameters

• Formula: C30 H49 N Os Ru2
• Calculated formula: C30 H48 N Os0.99 Ru1.98
• SMILES: [Ru]123456(N([Os]789%10%11([H]5)[c]5([c]7([c]8([c]9([c]5%10C)C)C)C)C)[Ru]5789([H]6)([H]%11)[c]6([c]5([c]7([c]8([c]69C)C)C)C)C)[c]5([c]1([c]2([c]3([c]45C)C)C)C)C
• Title of publication: Heterometallic Effects in Nitrogen‒Hydrogen Bond Cleavage by Trinuclear Mixed-Metal Polyhydrido Clusters Containing Ruthenium and Osmium
• Authors of publication: Kameo, Hajime; Nakajima, Yumiko; Namura, Kyo; Suzuki, Hiroharu
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 24
• Pages of publication: 6703
• a: 11.092 ± 0.005 Å
• b: 15.476 ± 0.006 Å
• c: 15.867 ± 0.005 Å
• α: 138.821 ± 0.009°
• β: 108.491 ± 0.015°
• γ: 91.926 ± 0.016°
• Cell volume: 1530.5 ± 1.2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No