Information card for entry 4067807

Structure parameters

• Formula: C61 H70 Cl10 P4 Pd Rh2
• Calculated formula: C61 H68 Cl10 P4 Pd Rh2
• SMILES: [Pd]1(Cl)(Cl)[P](C[P]([Rh]2345(Cl)(Cl)[c]6([c]2([c]3([c]4([c]56C)C)C)C)C)(C[P]1(C[P]([Rh]1234(Cl)(Cl)[c]5([c]1([c]2([c]3([c]45C)C)C)C)C)(c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.ClCCl.ClCCl
• Title of publication: Heterotrinuclear Complexes with Palladium, Rhodium, and Iridium Ions Assembled by Conformational Switching of a Tetraphosphine Ligand around a Palladium Center
• Authors of publication: Yoshii, Akiko; Takenaka, Hiroe; Nagata, Hiroko; Noda, Sayo; Nakamae, Kanako; Kure, Bunsho; Nakajima, Takayuki; Tanase, Tomoaki
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 1
• Pages of publication: 133
• a: 23.354 ± 0.005 Å
• b: 15.269 ± 0.003 Å
• c: 18.148 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6471 ± 2 ų
• Cell temperature: 168 ± 2 K
• Ambient diffraction temperature: 168 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for all reflections included in the refinement: 0.0959
• Goodness-of-fit parameter for all reflections included in the refinement: 1.243
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No