Crystallography Open Database

Information card for entry 4069007

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Structure parameters

Formula	C57 H59 B2 F8 O5 P4 Rh2
Calculated formula	C57 H59 B2 F8 O5 P4 Rh2
Title of publication	Asymmetric Hydrogenation. Dimerization of Solvate Complexes: Synthesis and Characterization of Dimeric [Rh(DIPAMP)]22+, a Valuable Catalyst Precursor
Authors of publication	Preetz, Angelika; Baumann, Wolfgang; Fischer, Christian; Drexler, Hans-Joachim; Schmidt, Thomas; Thede, Richard; Heller, Detlef
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	13
Pages of publication	3673
a	13.261 ± 0.003 Å
b	20.409 ± 0.004 Å
c	21.194 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	5736 ± 2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	20
Hermann-Mauguin space group symbol	C 2 2 21
Hall space group symbol	C 2c 2
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0307
Weighted residual factors for significantly intense reflections	0.0524
Weighted residual factors for all reflections included in the refinement	0.0543
Goodness-of-fit parameter for all reflections included in the refinement	0.891
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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