Information card for entry 4069009

Structure parameters

• Formula: C28 H38 B Cl F4 N2 Pd Ru
• Calculated formula: C28 H38 B Cl F4 N2 Pd Ru
• Title of publication: Bimetallic η6,η1NCN-Pincer Ruthenium Palladium Complexes with η6-RuCp Coordination: Synthesis, X-ray Structures, and Catalytic Properties⊥
• Authors of publication: Bonnet, Sylvestre; van Lenthe, Joop H.; Siegler, Maxime A.; Spek, Anthony L.; van Koten, Gerard; Gebbink, Robertus J. M. Klein
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 7
• Pages of publication: 2325
• a: 14.1334 ± 0.0005 Å
• b: 14.7569 ± 0.0005 Å
• c: 16.1141 ± 0.0006 Å
• α: 78.019 ± 0.002°
• β: 77.718 ± 0.002°
• γ: 63.285 ± 0.002°
• Cell volume: 2909.14 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0959
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for significantly intense reflections: 0.1103
• Weighted residual factors for all reflections included in the refinement: 0.1282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No