Crystallography Open Database

Information card for entry 4069053

Preview

Coordinates	4069053.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59 H81 B O Os2 Ru
Calculated formula	C58.47 H65.41 B O Os2 Ru
Title of publication	Synthesis of Heterometallic Trinuclear Polyhydrido Clusters Containing Ruthenium and Osmium and Their Electronic and Structural Deviation from Homometallic Systems
Authors of publication	Kameo, Hajime; Shima, Takanori; Nakajima, Yumiko; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	8
Pages of publication	2535
a	10.5705 ± 0.0003 Å
b	14.6098 ± 0.0005 Å
c	17.4238 ± 0.0007 Å
α	85.321 ± 0.0012°
β	87.989 ± 0.001°
γ	88.838 ± 0.0009°
Cell volume	2679.78 ± 0.16 Å³
Cell temperature	163 ± 2 K
Ambient diffraction temperature	163 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0394
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.086
Weighted residual factors for all reflections included in the refinement	0.0895
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069053.html